Abstract
Triple-decker complexes with a bridging borole ligand (C 4H 4BPh)Rh(μ-C 4H 4BPh)ML (ML = RuCp, 2a; RuCp ∗, 2b; FeCp ∗, 3; Co(C 4Me 4), 4; Ir(cod), 5) were synthesized by stacking reactions of [Rh(C 4H 4BPh) 2] − ( 1) with cationic [ML] + fragments. The structures of 2a, b and (C 4H 4BPh)Rh(μ-C 4H 4BPh)Rh(C 4H 4BPh) ( 6) were determined by X-ray diffraction.
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