Abstract
1-β-Telluroglycosides isomerize to α-isomers upon photolysis and thermolysis. The isomerization follows first-order reaction kinetics and proceeds through a glycosyl radical intermediate by homolytic CTe bond cleavage. The radicals so generated are trapped intermolecularly by TEMPO free radical, indicating that the glycosyl radicals are efficiently generated by a non-chain mechanism.
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