Abstract
In the paper the evolution characteristics of structural properties of zinc oxide powders produced by mechanical milling in a high-energy attritor using Raman spectroscopy are studied. Milling time was 1, 3 and 5 h. It is found that the main spectral change observed in the Raman spectra of the samples, is a monotonic intensity increase of E1(LO)x mode associated with increasing concentrations of defects in the material.
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