Research into mechanical properties of reaction-bonded SiC composites at cryogenic temperatures

Abstract

The mechanical properties of reaction-bonded silicon carbide (RBSC) composites at cryogenic temperatures have been reported for the first time. The results show that the flexural strength and fracture toughness increase from 277.93 ± 23.21 MPa to 396.74 ± 52.74 MPa and from 3.69 ± 0.45 MPa·m 1/2 to 4.98 ± 0.53 MPa·m 1/2 as the temperature decreases from 293 K to 77 K, respectively. The XRD analysis of the phase composition reveals that there is no phase transformation in the composites at cryogenic temperatures, indicating cryogenic mechanical properties are independent of phase composition. The enhancement of mechanical properties at 77 K over room temperature could be explained by the transition of fracture mode from predominant transgranular fracture to intergranular fracture and stronger resistance to crack propagation resulting from higher residual stress at 77 K. The above results demonstrate that such composites do not undergo similar deteriorations in the fracture toughness as other materials (some kinds of metals and polymers), so it is believed that such composites could be a potential material applied in cryogenic field.