Abstract
Radioactive sodium is removed from Experimental Breeder Reactor-II components by immersing the components in denatured alcohol until the sodium has reacted with the alcohol. The resulting radioactive sodium-alcohol solution must be processed to separate and convert the sodium to a solid waste for disposal. A process was developed and is described that converts radioactive sodium dissolved in alcohol to a dry powdered carbonate waste product and recovers the alcohol for reuse. The sodium-alcohol waste solution, after adjustment for proper sodium and water content, is fed to a wiped-film evaporator operated at 190°C and maintained with a CO2 atmosphere that converts the dissolved sodium to anhydrous Na2CO3. The end product, ∼85 to 90 wt% Na2CO3, is directed into a 208-ℓ (55-gal) drum for disposal. Alcohol distilled during the process is condensed, collected, and dried for immediate reuse. The composition of the alcohol is not altered in the process.
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