Abstract

A countercurrent centrifugal extractor with an inner rotor and a stationary outer wall has been developed in which aqueous and organic phases flow countercurrently between two walls. The formation of stable Taylor vortices in the gap makes multistage extraction possible. Understanding the relation between flow state and percent extraction is important for achieving a greater number of theoretical stages in a single extractor. Hence, oil–water countercurrent flow is measured by ultrasonic velocity profiling, without disturbing the flow, under different feed rates of solutions and rotating speeds of the inner rotor. In continuous extraction tests, Zn2+ in nitric acid and di-(2-ethylhexyl)-phosphoric acid diluted by n-dodecane are used. Measurement results are verified by numerical simulation. Finally, a correlation chart of flow patterns and operating conditions is prepared.

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