Abstract
We have reinvestigated the dilacunary 19‐tungsto‐2‐arsenate(III) [AsIII2W19O67(H2O)]14– (1), resulting in the mixed potassium–sodium salt K8Na6[AsIII2W19O67(H2O)]·28H2O (KNa‐1), which was structurally characterized in the solid state by single‐crystal XRD, IR, TGA, and elemental analysis, as well as in aqueous solution by 183W NMR spectroscopy for the first time.
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