Abstract
Glycidyl esters in the presence of trifluoroacetic anhydride (TFAA) and trimethylsilyl halides (TMSX), undergo a regioselective opening of the oxirane system with a subsequent migration of the acyl group to afford 1-trifluoroacetyl-2-acyl-3-haloglycerols. From these, the corresponding 2-acyl-3-haloglycerols can be obtained quantitatively and in high purity (>99%) without chromatographic purification.
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