Abstract
Refinement of the crystal structure of arsenic tribromide is reported.13; A single crystal of arsenic tribromide was obtained by crystallizing13; the specimen in a sealed thin-walled capillary tubel (radius 0.31 mm).13; The intensity data were collected using equi-inclination Weissenberg13; technique. The intensities were measured visually and corrected for13; absorption and Lorentz-polarisation factors.13; The coordinates reported by SINGH and SWA1\UNATHAN2gave an13; R factor of 0.26. Further refinement by the method of least squares13; was attempted on the Elliott 803B computer. The analytical expression13; of FORSYTH and WELLS3 was used for atomic scattering factors.13; Only individual isotropic temperature factors were used. After four13; cycles of refinement the R factor dropped to 0.143. No attempt was13; made to apply anisotropic temperature factors.
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