Abstract
AbstractTriplet dioxygen was reduced by TEMPO or trityl radicals in the presence of two molar equivalents of the strong B(p‐C6F4X)3 (X: F or H) boron Lewis acids under mild conditions to give the bis(borane)superoxide systems 2. The sensitive radical anion species were isolated and characterized by methods including X‐ray crystal structure analysis and EPR spectroscopy.
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