Reduced leakage current of multiferroic BiFeO3 ceramics with microwave synthesis

Abstract

Preparation of multiferroic BiFeO3(BFO) is reported using microwave heating. The prepared sample is characterized using x-ray diffraction, scanning electron microscopy, differential scanning calorimetry and leakage current measurements. It is observed that the BFO can be prepared with microwave heating at a fast heating rate, consisting of more homogeneous microstructure and better electrical properties. Phase purity of the sample is confirmed from x-ray diffraction measurements. Uniform grain size distribution is observed for the sample prepared with microwave heating. More than an order of magnitude reduction in the leakage current is observed for the sample prepared with microwave heating as compared to conventional radiant heating.