Abstract
The crystal structure of the title compound, (C24H20As)[ReCl4O(H2O)], has been re-examined at 100 K. The complex contains distorted octahedral [ReOCl4(H2O)]− anions, with the Re atom and disordered aqua ligand located on a fourfold axis, and [Ph4As]+ cations with the As atom located on a fourfold inversion axis. In the anion, the terminal Re=O bond, 1.662 (2) Å, is trans to the aqua ligand and the Re—(OH2) and Re—Cl distances are 2.325 (3) and 2.3479 (5) Å, respectively.
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