Abstract

Large area graphene-poly (methyl methacrylate) (PMMA) closed cavity resonator has been fabricated. The resonator has been formed by transferring an ultra-large graphene-PMMA membrane over 3.5 mm diameter circular closed cavity with $220~\mu \text{m}$ depth. The graphene-PMMA membrane includes 6-layer graphene and 450 nm PMMA film. A modified graphene-PMMA dry transfer method has been developed in this work. Using the Kapton tape supporting frame, the graphene-PMMA membrane has been dry transferred onto the substrate with a small membrane’s static deformation of around 180 nm. The membrane’s static deformation aspect ratio (suspended membrane’s diameter over the membrane’s deformation) is around 19,500. The graphene-PMMA closed cavity resonator has been actuated mechanically, acoustically and electro-thermally. The dynamic behaviour of the membrane suspended over the closed cavity shows that the (1, 1) mode dominates the graphene-PMMA membrane’s resonance with a resonant frequency of around 10 kHz and suggests the device is under good gas encapsulation. Acoustic vibration amplitude sensitivity of graphene-PMMA membrane over the closed cavity is measured to be around $6~\mu \text{m}$ /Pa. The membrane’s dynamic behaviour, simulated under similar mechanical and electro-thermal actuation conditions, has been shown to be consistent with the trend of the device’s experimental results. The strain in the suspended graphene-PMMA membrane is estimated to be 0.04 ± 0.01 %.

Highlights

  • M ECHANICAL graphene resonators in the micro- and nano- scale have been reported to possess outstanding properties, including ultralow mass, high quality factorManuscript received December 18, 2019; accepted December 28, 2019

  • Raman spectrum confirms that the ultra large graphene membrane has been transferred safely using the modified graphene dry transfer method

  • The WLI results indicate that the dry transfer method can be used to transfer graphenePMMA membrane over the large area closed cavity with small static deformation

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Summary

Introduction

M ECHANICAL graphene resonators in the micro- and nano- scale have been reported to possess outstanding properties, including ultralow mass, high quality factorManuscript received December 18, 2019; accepted December 28, 2019. M ECHANICAL graphene resonators in the micro- and nano- scale have been reported to possess outstanding properties, including ultralow mass, high quality factor. Date of publication January 13, 2020; date of current version April 3, 2020. The associate editor coordinating the review of this article and approving it for publication was Dr Carlos Marques. Some graphene-based acoustic sensors with good performance, including microphones, open cavity resonators and loudspeakers, have been fabricated successfully in the past [9]–[15]. Such devices have graphenebased membrane aspect ratios, defined as the diameter to thickness ratio for the membrane, between 3400 and 350,000

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