Abstract

Laser cleaning is a competitive alternative to ablate and remove the hard oxide layer on hot-rolled stainless steel. To meet the practical demand, laser-induced breakdown spectroscopy (LIBS) was applied for real-time monitoring of the cleaning process in this study. Furthermore, the as-received and laser cleaned surfaces were characterized by an optical micrograph, an X-ray diffractometer, and a laser scanning confocal microscope. The results showed the relative intensity ratio (RIR) of the FeI emission line at 520.9 nm and the CrI emission line at 589.2 could be a quantitative index to monitor the cleaning process. When the oxide layer was not fully cleaned, the LIBS signals of the substrate were not excited, and the ratio was almost invariant as the power of the laser increased. However, it sharply increased once the oxide layer was effectively cleaned, the cleaned surface was bright, and the surface roughness was smaller in this case. Subsequently, as the surface was over-cleaned with the further increase of laser power, the RIR value remained large. The optimal laser cleaning parameters obtained by the monitoring were determined to avoid re-oxidation and reduce the roughness of the cleaned surface.

Highlights

  • Ra at three parallel lines filometer obtained by Laser scanning confocal microscope (LSCM), the average surface roughness Ra at three parallel lines was was calculated by software directly

  • To ablate the oxide layer on the hot-rolled stainless steel, laser cleaning technology coupled with real-time laser-induced breakdown spectroscopy (LIBS) monitoring was adopted in this study

  • The relative intensity ratio (RIR) of the FeI -520.9 and CrI -589.2 obtained by the monitoring was closely related to the cleaning of the oxide layer on the hot-rolled stainless steel

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Summary

Introduction

Publisher’s Note: MDPI stays neutral with regard to jurisdictional claims in published maps and institutional affiliations. Compared to low-alloy steel, the oxide layer on the stainless steel is so tightly connected with the substrate that only mechanical shot peening or strong acid pickling can be applied to remove it in the industry [3,4]. In this process, the efficiency of cleaning is low and the degree of environmental pollution is great. The aim was to provide a way for the real-time optimization of parameters during laser cleaning of the oxide layer on hot-rolled stainless steel and promote the application of laser cleaning in this field

Sample Preparation
Laser Processing and Real-Time Monitoring
50 HCl mL HCl
Optical Spectra During Laser Cleaning
Characterization of morphologies themorphologies
O4 and Cr2because ing was conducted atproducts
4.1.Discussion
The Mechanism of Laser Cleaning
Conclusions
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