Abstract
Reactions of N-acetyltrifluoroacetamide with chlorophosphites give rise to O-phosphorylated N-trifluoroacetoacetylimidates, which transform into α-phosphorylated vinylamides of trifluroacetic acid as a result of vinylphosphite-vinylphosphonate rearrangement. On the basis of nonempirical calculations data the reaction protocol of N-acetyltrifluoroacetamide with chlorophosphites was suggested.
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