Abstract
AbstractCysteine sulfenyl thiocyanate (CSSCN) reacts with thiols at pH 0 to cleanly yield disulfides. 2‐Mercaptoethanol (2‐MESH), 3‐mercaptopropionic acid (3‐MPASH), penicillamine (PENSH), and glutathione (GSH) react with CSSCN to give the corresponding mixed disulfides: 2‐MESSC, 3‐MPASSC, PENSSC, and GSSC. These compounds are stable at pH 0 and have been characterized by 1H and 13C NMR spectroscopy. © 2007 Wiley Periodicals, Inc. 18:467–471, 2007; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20340
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