Abstract
A method has been developed for the perfluoroalkylation of mercaptopolychloropyridines by the thermolysis of xenon(II) perfluoroalkanecarboxylates, obtained by the reaction of xenon difluoride and aperfluoroalkanecarboxylic acids, in the presence of the appropriate thiol. Perfluoroalkylthio derivatives of polychloropyridines have been synthesized. The fluorosulfonyl derivatives of tetrachloropyriidne and of tetrachloropyridine N-oxide were obtained by the action of XeF2 on mercaptotetrachloropyridine dissolved in aqueous HF.
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