Abstract
Ph4Sb[OC(Me)CHC(O)(O)CCH(Me)CO]SbPh4, a binuclear chelate complex, has been synthesized by a reaction between pentaphenylantimony and octanetetraone-2,4,5,7 (2: 1 mol/mol) in toluene. The Sb(1,2) atoms each have a distorted octahedral coordination, the CSbC and CSbO trans-angles lie within a range of 158.3(8)°–169.1(9)°, and the Sb-C bond lengths are 2.06(2)–2.25(2)A. The two six-membered [SbO2C3] chelate rings have the following distances (A): Sb-O, 2.25(1)–2.29(1); O-C, 1.20(2)–1.32(2); C-C, 1.32(3)–1.53(3).
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