Abstract
AbstractAn efficient and rapid method of synthesizing 1–3,3‐dimethyl triazenes has been developed. This method involves utilizing in situ generated aryldiazonium tetrafluoroborate salts using substituted aryl amines with “DMF‐DMA” (N,N‐Dimethylformamide‐dimethyl acetal) at room temperature. This reaction achieved good to excellent yields (68–95 %) under ambient conditions with a significantly faster rate. The proposed reaction was screened with various withdrawing, donating, and neutral groups containing aryldiazonium salts, and obtained products were confirmed by 1H, 13C NMR and mass spectroscopy techniques.
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