Abstract
Procedure for 107Pd determination in radioactive wastes coming from decommissioning of NPP A-1 is proposed and verified. 107Pd was separated and purified by Pd precipitation with dimethylglyoxime (DMG) and/or ferric hydroxide precipitation. 107Pd yield was determined gravimetrically by weighing the Pd(DMG)2 precipitate. 107Pd counting was performed using liquid scintillation counter (LSC-TDCR) and scintillation cocktail Hionic Fluor. In all analyzed samples the determined activities of 107Pd were lower than MDA. Nevertheless such analyses permit the decision concerning the storage of solidified wastes in the Mochovce regional repository.
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