Abstract
A rapid and accurate method for the determination of fluorine in organic compounds has been developed. The sample is decomposed by a Schöniger oxygen flask combustion and the liberated fluoride is determined by the thorium chloranilate method. The standard deviation of the procedure is ±0.12%, and it may be applied to samples in the 1–5 mg. range. The procedure is rapid. An analyst can complete 12–16 samples a day with ease.
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