Abstract
Abstract In this work, anatase-type TiO2 layers were prepared by deposition of precursor solution including titanium isopropoxide, ethanol and acetic acetylacetone on a FTO substrate using rapid expansion of supercritical solutions (RESS). The spraying to obtain a particulate coating of TiO2 was carried out at 65 °C and 180 bar of supercritical carbon dioxide environment. Then, thermal annealing at 550 °C for 2 h was applied to coated substrates to obtain desired phase composition. The structural and optical properties of the film were evaluated by XRD, SEM and UV-Vis. SEM observation showed that the photoanode film has porous microstructure with interconnected spherical TiO2 grains. TiO2 film has a band gap of 2.6 eV.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
