Abstract
A new method for rapid quantitative analysis of cellulose in viscose has been developed. The method is to regenerate cellulose in viscose by use of ammonium chloride and hydrochloric acid, the regenerated cellulose is separated by centrifuging, taken up in sulfuric acid, oxidized with an excess of potassium dichromate solution and the excess of the dichromate is back titrated with the standard ferrous ammonium sulfate solution with the use of barium salt of diphenylamine as an internal indicator. The time required for the analysis by this method is about one hour while it requires about hours by usual quantitative method.
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