Abstract
A flow-through apparatus with a microtube-reactor has been developed for rapid and continuous hydrothermal synthesis. Heat-up time of starting solution to 523 K is within 0.08 s and this promises rapid nucleation of nanoparticles compared with conventional batch reactor. Continuous production of Ag, Fe 2O 3, TiO 2, and ZrO 2 particles from metal salts aqueous solution was performed at 523 K and 30 MPa with the reactor. Nanoparticles having an average particle size and a coefficient of variation less than 5.4 nm and 0.22 could be continuously obtained.
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