Abstract
To better understand radiochemical reactions in the process of tritium recovery from the in-vessel components of future deuterium–tritium fusion machines like international thermonuclear experimental reactor (ITER), reactions in a N 2-balanced system of tritium oxides (T 2O and possible T 2O 2) with carbon monoxide (CO) were examined by laser Raman, Fourier transform infrared (FT-IR) and mass spectrometry. The main products after the reactions were completed at 290 K are carbon dioxide (CO 2) and tritiated water (T 2O). Tritiated acids as found in T 2–CO system were not detected in the reactions between T 2O/T 2O 2 and CO at the same detection limit.
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