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Abstract
Radiolysis of frozen aqueous or methanolic glasses containing sodium borohydride gave E.S.R. features characteristic of ·BH 3 − as the major radical product. These radicals were strongly associated with the solvent lattice in contrast with their behaviour in the parent salt. Additional E.S.R. features separated by ca. 200 G are assigned to BH 4, but since this spectrum could never be obtained in the absence of the intense BH 3 − features, this assignment is tentative.
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