Abstract
Abstract A LC/TSP/MS/MS selected reaction monitoring (SRM) method in the daughter ion scan mode can be succesfully applied for the quantitative determination of members of the Thioxanthenegroup like Chlorprothixene, Flupenthixol, Thiothixene and Zuclopenthixol in whole-blood following a BondElut extraction. Detection limits as low as 100pg for Chlorprothixene varying to 2ng per injection for the other compounds were found (corresponding to 0.5 to 10ng per mL whole-blood). Sensitivity of the proposed method is of the same order of chromatographic methods with other detectors or a RIA method.
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