Abstract
A GLC assay was developed for the determination of oxycodone levels in human plasma using a nitrogen-specific detector. The assay was developed for use in bioavailability studies of therapeutic doses of oxycodone. After ingestion of a commercial tablet containing 4.5mg of oxycodone hydrochloride and 0.38mg of oxycodone terephthalate by six volunteers, the mean peak oxycodone concentration in plasma was 18.4ng/ml at 1hr.
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