Abstract
The possibility of determining alunite by the derivatographic method according to the area of desulphurization endoeffect on the DTA curve and corresponding to this effect the weight loss on the TG curve has been investigated. It has been proposed to carry out the determination by the calibration curve constructed for standard samples and their area of endoeffect and by the weight loss depending on the content of alunite in the samples, since the dissociation of sulfur bound from 4500C accompanies the whole process. The analysis of samples should be carried out at an intensity of temperature increase of 100C/min, since at an intensity of 300C/min. the peak area increases significantly, and the indicators are not stable. It has been shown that the analyses in an inert medium lead to a twofold loss of sulphur bound, in contrast to the air medium, before desulphurization till the formation of the endoeffect
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
