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Abstract
The synthesis of protoporphyrin-I dimethyl ester (2)via the b-oxobilane route is reported. Fractional crystallisation was unsuccessful in the separation of the dimethyl esters of protoporphyrin-I and protoporphyrin-IX and also the tetramethyl esters of coproporphyrins -I and -III; the significance of these observations, in relation to biosynthetic investigations, is discussed.
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Schedule a callMore From: Journal of the Chemical Society, Perkin Transactions 1
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