Abstract
In the title compound, C33H29NO2, the central pyridyl ring makes dihedral angles of 42.71 (16), 44.78 (16), 85.47 (12) and 76.74 (12)° with the four phenyl rings. There are two intramolecular O—H⋯N hydrogen bonds. In the crystal structure, molecules are linked into a chain running along the b axis by a weak C—H⋯π interaction.
Highlights
Structure Reports OnlineKey indicators: single-crystal X-ray study; T = 291 K; mean (C–C) = 0.006 A; R factor = 0.054; wR factor = 0.127; data-to-parameter ratio = 8.9
In the title compound, C33H29NO2, the central pyridyl ring makes dihedral angles of 42.71 (16), 44.78 (16), 85.47 (12) and 76.74 (12) with the four phenyl rings
Molecules are linked into a chain running along the b axis by a weak C—HÁ Á Á interaction
Summary
Key indicators: single-crystal X-ray study; T = 291 K; mean (C–C) = 0.006 A; R factor = 0.054; wR factor = 0.127; data-to-parameter ratio = 8.9. C33H29NO2, the central pyridyl ring makes dihedral angles of 42.71 (16), 44.78 (16), 85.47 (12) and 76.74 (12) with the four phenyl rings. There are two intramolecular O—HÁ Á ÁN hydrogen bonds. Molecules are linked into a chain running along the b axis by a weak C—HÁ Á Á interaction. Related literature For organometallic pincer complexes, see: Dupont et al (2005); Gauvin et al (2001); Haenel et al (2001); van der Boom & Milstein (2003); van der Boom et al (1997); Vigalok & Milstein (2001); Bergbreiter et al (1999). The title compound was prepared according to the procedure described by Berg & Holm (1985)
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