Abstract
The solvent extraction of iron and titanium from coal fly ash leach solution was investigated by the use of Design of Experiments. The effect of the factors: hydrogen ion concentration, Primene JMT concentration, aqueous to organic volume phase ratio and temperature on iron and titanium extraction were evaluated. A two level factorial design implemented by statistical software Design Expert® 6, determined the significant factors and any associated interactive effects amongst these factors.Hydrogen ion concentration and the interaction between the aqueous to organic volume phase ratio with Primene JMT concentration had a significant effect on the extraction of iron while temperature did not. Hydrogen ion concentration and temperature did not have a significant effect on the extraction of titanium, while the interaction between Primene JMT concentration and the aqueous to organic volume phase ratio had a significant effect.The maximum iron extraction achieved in the implemented design was 33.8% while 99% of titanium could be extracted from the coal fly ash leach solution. Extraction improvement tests showed that at a hydrogen ion concentration of 0.28M, 88% iron and 99% titanium extraction from coal-fly ash leach solution could be achieved.
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