Abstract
AbstractThe synthesis of isothiocyanates (ITCs) by employing polymer‐supported 1,4,2‐oxathiazoles is described. The ITCs are obtained in moderate yields and high purity through a reagentless, thermal fragmentation of polymer‐supported 1,4,2‐oxathiazoles that are obtained by trapping nitrile oxides with polymer‐supported thiocarbonates.
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