Abstract

The results of a systematic, micro-scale experimental investigation on two-phase gas/brine flow through proppant-packed fractured shale samples under increasing effective stresses of up to 5000 psi are presented in this paper. We use a miniature core-flooding apparatus integrated with a high-resolution X-ray micro-CT scanner to perform the flow experiments. Geomechanical deformation and its impact on displacement mechanisms governing fluid transport within the packed fractures are studied at the pore scale under certain flow and stress conditions. These conditions were carefully designed to represent reservoir depletion and transport of water through such media. Since proppant grains are placed to maintain the long-term conductivity of the induced fractures, they significantly influence the geomechanical and multi-phase flow behavior of these conduits during reservoir depletion. We particularly examined the effectiveness of modified resin-coated sand (compared to a basic white sand) in maintaining the hydraulic conductivity of induced fractures. Significant bullet-like embedment and proppant crushing under severe stress conditions were found to be the shortcomings of these proppants, respectively. We then developed a methodical framework to design improved proppants with a similar mechanical strength to the host shale rock to withstand these drawbacks.Sphericity, roundness, and size of the proppant grains also impacted the critical properties of the constructed pore space such as pore size distribution and pore-throat aspect ratio. Such parameters control pore-scale gas-to-brine and brine-to-gas displacements within the hydraulic fractures. We specifically studied the non-wetting phase trapping and its subsequent impact on reduction of available pore space for other fluids to flow. It was found that trapped gas globules are very likely to deform within the medium and redistribute/reconnect under a higher effective stress. For the first time, wettability alteration of the proppant pack from water-wet to oil-wet was observed in a gas/brine fluid system. Wettability alteration occurred non-uniformly and was thought to be due to deposition of the shale organic matter released after significant proppant embedment. Such wetting characteristics aggravate multi-phase trapping within the fractures, which in turn leads to dramatic reductions in effective gas permeability. This study is concluded with a set of recommendations that can be used to effectively maintain the productivity of propped fractures for extended period of time.

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