Abstract
1. Titanium perchlorate in anhydrous perchloric acid medium with the formation of cesium hexaperchloratotitanate Cs2 [Ti(ClO46)]. Complexes with a ratio CsClO4:Ti(ClO4)4>2 are not formed. 2. On the basis of the IR spectra, a conclusion was drawn on a change in the mode of coordination of the perchlorato groups from bidentate in the Ti(ClO4)4 molecule to monodentate in the [Ti(ClO4)6]2− anion.
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