Abstract

Stainless steel fibres (SSF) were first wound and then plated with electrical nickel film. Alternative layers of these properly spaced Ni-coated stainless steel fibres (SSF–Ni) and aluminum foils were then stacked and diffusion bonded at 500 °C, 100 MPa in vacuum for 10 min to produce an SSF–Ni–Al precursor. Lower-temperature reactive hot pressing (RHP) at 700 °C, a process employed in this work, allowed the nickel and aluminum to react to form an NiAl matrix at a temperature approximately 500 °C lower than that accomplished by hot pressing, hot extrusion or hot isostatic pressing (HIP). RHP at 650 °C was also undertaken in order to investigate the mechanism leading to the formation of a nickel aluminide matrix composite. A dense specimen with complete NiAl reaction was obtained by hot pressing at 900 °C. The variance in microstructure that resulted from the different conditions of heat treatment and hot pressing was analysed by optical microscopy, scanning electron microscopy and X-ray diffraction (XRD).

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