Processing of Porous-Core Materials for Bone Implant Applications: A Permeability and Mechanical Strength Analysis

Abstract

This study presents a methodology to fabricate Ti6Al4V cylindrical compacts with a highly porous core and dense shell with the aim to mimic the bone microstructure. Compacts with different core diameters were obtained via conventional pressing and sintering. Large pores were created with the aid of pore formers. Dilatometry was used to determine the sintering kinetics, while X-ray computed tomography was used for characterization. Also, the permeability was evaluated on the 3D microstructure, and the mechanical strength was evaluated via compression tests. The results indicated that sintering was constrained by the different densification rates of the porous and dense layers. However, defect-free compacts were obtained due to neck bonding between the Ti6Al4V particles. Large pores were located in the designed core with a similar pore size distribution. The permeability increased following a power law as a function of the pore volume fraction. The porous core drove the stiffness of the bilayer components, while the combination of both layers increased their strength. The bilayer materials showed permeability (1.36 × 10−10 m2), mechanical properties (E = 6.83 GPa and σy = 299 MPa), and admissible strain (σy/E = 43 × 10−3) similar to those of human bones.