Abstract
• 1 H and 13 C NMR study of the role of water and DMF in UiO-66. • Hydrogen bonds are probed by solid-state NMR. • Selective deuteration of the Zr–OH groups to remove the 1 H– 1 H dipolar interaction. • Selective deuteration of the aromatic hydrogen atoms to remove the 1 H– 1 H dipolar interaction.
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