Abstract

Based on low-temperature high-permeability grain-oriented silicon steel designed with an initial nitrogen content of 0.0055% and produced by the thin slab casting and rolling process, the effect of total nitrogen content and nitriding temperature on primary recrystallization microstructure and texture were studied by optical microscope, scanning electron microscope, transmission electron microscope, and electron backscatter diffraction. The nitriding temperature affects the primary recrystallization behaviors significantly, while the total nitrogen content has a small effect. As the nitriding temperature is 750–850 °C, the average primary grain size and its inhomogeneity factor are about 26.58–26.67 μm and 0.568–0.572, respectively. Moreover, the texture factor is mostly between 0.15 and 0.40. Because of the relatively sufficient inhibition ability of inherent inhibitors in a decarburized sheet, the nitriding temperature (750–850 °C) affects the primary recrystallization microstructure and texture slightly. However, as the nitriding temperature rises to 900–950 °C, the average primary grain size and its inhomogeneity factor increase to 27.75–28.26 μm and 0.575–0.578, respectively. Furthermore, because of the great increase on the area fraction of {112} <110> grains, part of texture factor is increased sharply. Therefore, in order to obtain better primary grain size and homogeneity, better texture composition, and stability of the decarburized sheet, the optimal nitriding temperature is 750–850 °C.

Highlights

  • High-permeability grain-oriented silicon steel (Hi-B) is one of the most important functional materials in the development of the power industry and is widely used as a core material for transformers

  • Based on the faster solidification speed, lower soaking temperature, and shorter soaking time of a thin slab, utilizing the thin slab casting and rolling process (TSCR) process is extremely beneficial in controlling the size and distribution of inherent inhibitors and in forming fine and uniform primary recrystallization grains after decarburization annealing for Hi-B steel production [13,14]

  • As the total nitrogen content is in the range of 0.007– 0.026%, the average grain sizes of primary recrystallization are 25.4–28.2, 25.9–27.8, 25.6– 27.2, 27.1–28.6, and 27.1–28.7 μm, respectively

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Summary

Introduction

High-permeability grain-oriented silicon steel (Hi-B) is one of the most important functional materials in the development of the power industry and is widely used as a core material for transformers. Based on the faster solidification speed, lower soaking temperature, and shorter soaking time of a thin slab, utilizing the TSCR process is extremely beneficial in controlling the size and distribution of inherent inhibitors and in forming fine and uniform primary recrystallization grains after decarburization annealing for Hi-B steel production [13,14]. It will help employ a lower nitrogen content design for the composition of Hi-B steel, which makes the precise control of nitrogen in the refining process relatively easy, and the production cost will be reduced. It is expected to provide a reference for the production of low-temperature Hi-B steel by the TSCR process, especially for the design and optimization of the nitriding process

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