Abstract

The thin-walled airfoil areas of as-cast single-crystalline turbine blades made of CMSX-4 superalloy were studied. The blades were produced by the industrial Bridgman technique at withdrawal rates of 2, 3 and 4 mm/min. The angle between the [001] crystallographic direction and blade axis, related to the primary orientation, was defined by the Ω-scan X-ray diffraction method at points on the camber line located near the tip of an airfoil and at points of a line located in parallel and near the trailing edge. Additionally, primary crystal orientation was determined by Laue diffraction at the selected points of an airfoil. The influence of mould wall inclination on the primary crystal orientation of the thin-walled areas is discussed. The effect of change in the [001] crystallographic direction, named as “force directing”, was considered with regard to the arrangement of primary dendrite arms in relation to the trailing edge and the camber line. It was stated that when the distance between the mould walls is less than the critical value of about 1.5 mm the “force directing” increases as the distance between the walls of the mould decreases. The effect may be controlled by selecting an appropriate secondary orientation using a seed crystal in the blade production process. The model of dendrite interaction with the mould walls, including bending and “deflection”, was proposed.

Highlights

  • Single-crystalline superalloys are a group of materials characterized by increased strength properties, especially creep resistance at high operating temperatures

  • The aim of the study is to determine a distribution of the α angle describing the primary crystal orientation of thin-walled areas of as-cast single-crystalline turbine blade airfoils, and to analyse the relation between this distribution and the slope of mould walls in relation to the axis of blades obtained at different withdrawal rates

  • In airfoils’ thin-walled areas of single-crystalline blades made of CMSX-4 by the Bridgman technique at withdrawal rates of 2, 3 and 4 mm/min., the inclination of the mould walls to the blade axis changes the arrangement of the [001] crystallographic direction in relation to the blade axis

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Summary

Introduction

Single-crystalline superalloys are a group of materials characterized by increased strength properties, especially creep resistance at high operating temperatures. The crystal orientation, which depends on the parameters of directional crystallization and the geometry of the cast [5,6,7], have an important effect on the mechanical properties of single-crystalline superalloy casts [1,8,9], such as stress rupture life and elongation [10]. The tensile strength and creep resistance of the blades depend on the presence of low-angle boundaries [11] and the localisation of low-angle boundaries is related to the cast geometry. The residual stress in a sub-surface area that may be created during crystallization [12] may be related to the cast geometry. In thin-walled areas the Materials 2019, 12, 2699; doi:10.3390/ma12172699 www.mdpi.com/journal/materials

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