Abstract

Herein, we report a single step and a one pot by using spin coating method for the preparation of optically transparent superhydrophobic TEOS-silica composite films. Silica sols were prepared by keeping the molar ratio of TEOS/CH3OH/H2O (0.1 M NH4F) constant at 1:33.15:6.06, respectively. Increasing the silica content of the coating solution resulted in decreasing the transparency of the composite films from 93 to 84% (in references to 93% transmission defined by a plain glass substrate). The static water and hexadecane contact angle of transparent surfaces were found to vary between 65° and 170° (sliding angle < 3°) and 45° to 5° (sliding angle = 15°) depending on the silica content. The stability of the surface remained nearly constant for several months under stored at ambient conditions. The mechanical stability of the prepared of TEOS-silica composite was tested by scratching and adhesive tape test. For the chemical test applications, NaOH, HCl, and H2SO4 were used for the TEOS-silica composite films.

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