Preparation of niobium aluminide dispersion strengthened with niobium boride : T. Takahashi et al (Hyogo Prefecture Inst. of Industrial Research, Kobe, Japan), J. Japan Soc. Powder and Powder Metallurgy, vol 41, no 2, 1994, 166–169. (In Japanese)

Abstract

Spray formed T15 high speed steel (HSS) billets were deposited using a state-of-the-art twin-atomiser spray forming facility. The effects of post thermo-mechanical processing (hot isostatic pressing and hot forging) and heat treatment on the microstructure and mechanical properties were investigated. As-deposited billet has a density over 99.3% of the theoretical value and no measurable macro-segregation was observed. The microstructure consists of the equiaxed grains with mean size of ∼18 μm and MC- and M6C-type carbides non-uniformly distributed inside the grains and along the grain boundaries. After optimal thermo-mechanical processing and heat treatment, the microstructure was composed of equiaxed fine tempered martensites, and refined M6C and MC spherical carbides particles uniformly distributed along the grain boundaries and inside the grains. The hardness reached HRC68 after thermo-mechanical processing, and the corresponding impact toughness and bending strength reached 27 J/cm2 and 4600 MPa respectively. Although HIP cannot increase the bending strength significantly, it can effectively improve the impact toughness through refining and globurizing carbides.