Abstract
A novel simple process for preparing MoS 2 by a mechanochemical route under the normal temperature and pressure has been developed. In this method, the mechanochemical solid-state reaction was completed in a high-energy planetary ball mill filled with pure argon. The effects of milling time and speed were discussed and the product was characterized by XRD, DSC and TEM. It is found that the as-obtained samples are MoS 2 with short low stacked layers less than 10 nm, which have potential application in the highly active catalysts.
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