Abstract
Abstract Monophenylthallium(III) complexes with a Tl–I or Tl–SR bond were prepared in the presence of dibenzo-18-crown-6. These complexes are stable in the air and to heat to their melting points. In the hydrogen sulfide complex, ν(S–H) band was found at 2570 cm−1 and δ(Tl–SH) was observed at 1.15 ppm with 2J(Tl-SH) = 405 Hz in CH2Cl2 solution.
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