Abstract
We have prepared partially exchanged Hg β′-alumina from single crystal and polycrystalline Na and Ag β′-alumina using the conventional molten salt immersion method and a newly developed reflux ion exchange method. In the reflux method, the sample is continually bathed in pure HgCl 2. The reflux method caused much higher Hg(II) exchange than the conventional immersion method. In single crystals of Ag β′-alumina, about 91 mole% of the Ag(I) was replaced by Hg(II) after seven days of reflux exchange compared to 15 m/o exchange with the conventional immersion method.
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