Abstract
The Friedel–Crafts reaction of PCl3 and benzene in [BuPy]Cl–XAlCl3 ionic liquids (ILs) was investigated for clean synthesis of dichlorophenylphosphine (DCPP). A simple product isolation procedure was achieved, and the effect of ILs composition, reactant composition, reaction time and quantity of ILs on this reaction were studied. The [BuPy]Cl–XAlCl3 rendered this reaction green characteristics. A catalytic mechanism was proposed as well.
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