Abstract
Cubic Na3PS4 (c-Na3PS4), a high temperature phase of Na3PS4, is successfully prepared by liquid-phase shaking from Na2S and P2S5 in methyl acetate medium. The effects of the amount of solvents, Na2S and heat treatment on the formation of c-Na3PS4 are carefully investigated. In addition to c-Na3PS4, an unknown phase is also detected in the sample containing an excess amount of Na2S in the starting materials mixture.
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