Abstract
Two adenosine-containing asymmetrical dinucleoside triphosphates were synthesized via the P(V)–N activation method. The key adenosine 5ʹ-phosphoropiperidate intermediate was obtained by a redox condensation method. The reaction of adenosine phosphoropiperidate with uridine 5ʹ- and cytidine 5ʹ-diphosphates in the presence of 4,5-dicyanoimidazole (DCI) afforded the desired dinucleoside triphosphates in good isolated yields.
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