Preparation and vibrational spectra of various esters and chlorides of antimonous acid

Abstract

1. 2-Methoxy-, 2-methoxy-4-methyl-, 2-methoxy-5,5-dimethyl-, 2-chloro-, 2-chloro-4-methyl-, and 2-chloro-5,5-dimethyl-1,3,2-dioxastibinanes have been prepared. 2. The bands due to the group vibrations ν (Sb-O) and ν (Sb-Cl) have been identified in the infrared and Raman spectra of the acyclic and cyclic esters and chlorides of antimonous acid obtained.