Abstract
Chlorofullerene D2d-C84(23)Cl24 was prepared by chlorination of D2d-C84(23) with VCl4 or SbCl5 at 320–350 °C. An X-ray crystallographic study with the use of synchrotron radiation revealed the addition pattern of 24 Cl atoms stabilized by the formation of isolated C=C bonds and benzenoid rings on the carbon cage.
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